--- 美國SPEX CLP項目標(biāo)液 ---
ICP-MS干擾測試標(biāo)液A2
ICP-MS Interferents A2
元素:10000mg/L: Cl
2000mg/L: C
1000mg/L: Al, Ca, Fe, K, Mg, Na, P, S
20mg/L: Mo, Ti
基體:5% HNO3/tr HF
體積:125mL
編號:CL-INT-A2
用途:Claritas PPT 級,電感耦合等離子體質(zhì)譜儀(ICP-MS)分析用元素標(biāo)液。EPA合約實驗室CLP項目標(biāo)液。
證書:每份標(biāo)液都附有一份內(nèi)容詳細(xì)的標(biāo)準(zhǔn)物質(zhì)證書,證書報告標(biāo)液中多至68種痕量雜質(zhì)元素含量實際測量結(jié)果。
溯源:美國NIST SRM (Traceable by NIST SRM)
**應(yīng)用參考 · INSTRUCTION**
每次測試開始和結(jié)束驗證干擾和背景校正因子,另外每20個樣品必需進(jìn)行檢測。
標(biāo)液CL-INT-A2,稀釋10倍,為溶液A,標(biāo)液CL-INT-A2稀釋10倍再加標(biāo)液CL-INT-B4稀釋100倍后混合,為溶液AB。溶液A和溶液AB用于見的干擾檢測。一旦兩種溶液配制好,需連續(xù)分析,從溶液A開始。
標(biāo)液CL-INT-A2,稀釋10倍,為溶液A,標(biāo)液CL-INT-A2稀釋10倍再加標(biāo)液CL-INT-B3稀釋100倍后混合,為溶液AB。溶液A和溶液AB用于見的干擾檢測。一旦兩種溶液配制好,需連續(xù)分析,從溶液A開始。
CLP ISM 01.2 and ILM 05.2 & 05.3 Standards for ICP-MS
For verification of inter-element and background correction factors at the beginning and the end of each analysis run. In addition, a verification must be done after every 20th sample. Two solutions are required for the most common interference check: Solution A, the interferents alone (CL-INT-A2) and Solution AB, a combination of interferents (CL-INT-A2) and analytes (CL-INT-B3 or CL-INT-B4). Solution A is prepared by diluting CL-INT-A2 10-fold. Solution AB is prepared by diluting CL-INT-A2 10-fold and CL-INT-B3 or CL- INT-B4 100-fold; for example, 10 mL of CL-INT-A2 and 1 mL of CL-INT-B3 or CL-INT-B4 into a 100 mL volumetric flask, brought to volume with a matrix blank. Once prepared, the solutions should be analyzed consecutively, starting with Solution A.